Synthesis and characterization of complexes of vic-dioxime derivatives with transition metal


KAYA M., Demir I., YENİKAYA C.

ASIAN JOURNAL OF CHEMISTRY, cilt.20, sa.3, ss.2221-2228, 2008 (SCI İndekslerine Giren Dergi) identifier identifier

  • Yayın Türü: Makale / Tam Makale
  • Cilt numarası: 20 Konu: 3
  • Basım Tarihi: 2008
  • Dergi Adı: ASIAN JOURNAL OF CHEMISTRY
  • Sayfa Sayıları: ss.2221-2228

Özet

A novel vic-dioxime compound (H(2)L) and their transition metal complexes were synthesized for the first time. This compound, N-[(4-(2,4-dihyroxybenzylideneamino)naphthalen-1-yl)]-N'-hydroxy-2-(hydroxyimino)acetimidamide, have been synthesized by starting metarial of naphthalene. The complexes of nickel(II), copper(II) and cobalt(II) with H2L were prepared. The ligand and its metal complexes were charecterized FT-IR, UV, (1)H NMR, (13)C NMR, MS, elemental analysis and conductometric measurements.