TURKISH JOURNAL OF CHEMISTRY, cilt.25, sa.3, ss.305-310, 2001 (SCI-Expanded)
Boron is one of the least sensitive elements in atomic emission spectrometry. As various refractory substances interfere in the analysis and because of the low sensitivity, sample enrichment and the separation of the interfering matrix is needed. Methyl borate has many advantages because of its simple generation conditions and its stability in the absence of moisture. New procedures for the generation of methyl borate without using external heating have also been investigated to produce a more rapid determination of boron.