POLYMERS, cilt.18, sa.6, 2026 (SCI-Expanded, Scopus)
Fused deposition modeling/fused filament fabrication (FDM/FFF) enables architectural tailoring of mechanical response through layer configuration and multi-material manufacturing strategies. However, the combined effects of layer arrangement, infill ratio, and packing geometry in polymer-metal hybrid structures and interfacial load transfer mechanisms are still not sufficiently elucidated. In this study, the tensile behavior of single- and multi-material structures produced using PLA and 17-4 PH stainless steel filaments was systematically investigated. A total of 24 experimental parameter sets were created with four-layer configurations (PLA, 17-4 PH, PLA/17-4 PH/PLA, and 17-4 PH/PLA/17-4 PH), three infill ratios (20%, 60%, and 100%), and two packing patterns (linear and hexagonal); the samples were tested according to the ASTM D638 standard. Mechanical data were modeled using Response Surface Methodology (RSM) and ANOVA, and the developed regression models showed high accuracy (R-2 > 0.95). The findings showed that tensile and yield strength are primarily controlled by the layer arrangement, while infill ratio and infill pattern have a secondary effect. The highest strength was measured in 100% infill linear PLA samples (approximate to 10.35 MPa), and the lowest value was measured in 17-4 PH "green part" samples without sintering (approximate to 0.92 MPa). Hybrid structures exhibited intermediate performance in the range of 2.9-4.9 MPa. ANOVA results showed that the majority of the mechanical variance was explained by the layer arrangement (70-85% contribution), while infill ratio and infill pattern had a secondary effect. Fracture surface analyses showed that high performance was associated with homogeneous filament fusion and low porosity; Studies have confirmed that poor performance is associated with delamination and interfacial separation.