Nano-sized Spherical MgB2 Superconducting Powder Fabrication Using MHz Range Ultrasonic Spray Pyrolysis (USP) System

YAKINCI, MEHMET; AKSAN, MEHMET; BALCİ, YAKUP; ALTIN, SERDAR; ÖNAL, YUNUS; AYDOĞDU, YILDIRIM

doi:10.1007/s10948-010-0924-4

Nano-sized Spherical MgB2 Superconducting Powder Fabrication Using MHz Range Ultrasonic Spray Pyrolysis (USP) System

Atıf İçin Kopyala

YAKINCI M. C., AKSAN M. A., BALCİ Y., ALTIN S., ÖNAL Y., AYDOĞDU Y.

JOURNAL OF SUPERCONDUCTIVITY AND NOVEL MAGNETISM, cilt.24, ss.235-239, 2011 (SCI-Expanded)

Yayın Türü: Makale / Tam Makale
Cilt numarası: 24
Basım Tarihi: 2011
Doi Numarası: 10.1007/s10948-010-0924-4
Dergi Adı: JOURNAL OF SUPERCONDUCTIVITY AND NOVEL MAGNETISM
Derginin Tarandığı İndeksler: Science Citation Index Expanded (SCI-EXPANDED), Scopus
Sayfa Sayıları: ss.235-239
Gazi Üniversitesi Adresli: Evet

Özet

We have fabricated 40-150 nm sized MgB2 superconducting spherical powders by using a 2.4 MHz ultrasonic spray pyrolysis system and consecutive high temperature heating and powder collection chamber. Various chemical solutions, which contain Mg, B, de-ionized water, acetone and LAPSA in different concentrations and gas atmosphere, were used to obtain MgB2 superconducting powders. Microstructural, transport and magnetic characterizations of the powders were performed using XRD, SEM-EDX, R-T, M-H analysis and critical current density calculations, which is found in the range of 10(6) Acm(-2), indicating improved flux pinning properties.