Exploring quenching temperature variations in quenching and partitioning heat treatment: impact on wear resistance and microstructural evolution of ductile iron


NALÇACI B., YILMAZ T., Pehlivan C., GÜRAL A., ERDOĞAN M.

Canadian Metallurgical Quarterly, 2025 (SCI-Expanded) identifier

  • Yayın Türü: Makale / Tam Makale
  • Basım Tarihi: 2025
  • Doi Numarası: 10.1080/00084433.2025.2490405
  • Dergi Adı: Canadian Metallurgical Quarterly
  • Derginin Tarandığı İndeksler: Science Citation Index Expanded (SCI-EXPANDED), Scopus, Aerospace Database, Chemical Abstracts Core, Communication Abstracts, Compendex, INSPEC, Metadex, Civil Engineering Abstracts
  • Anahtar Kelimeler: Ductile iron, martensite, multiphase, quenching and partitioning, wear
  • Gazi Üniversitesi Adresli: Evet

Özet

The present study was designed to investigate the effects of different quenching temperatures on the microstructure and wear resistance of Ductile Iron (DI) subjected to the Quenching and Partitioning (Q&P) heat treatment process. For this purpose, DI samples were cast into Y-block sand molds, and heat treatment studies were conducted on both wear test specimens and reference samples extracted from the Y-blocks. Following austenitizing at 900°C for 20 minutes, the samples were quenched at 110°C, 135°C, and 160°C for 5 minutes. Subsequently, a partitioning process was applied at 345°C for 60 minutes, followed by air cooling. The microstructural and mechanical characterisations of the samples were carried out using a ball-on-disc tribometer, hardness testing, X-Ray diffraction (XRD) analysis, optical microscopy, Scanning Electron Microscopy (SEM), and optical profilometry. The Q&P-treated DI samples exhibited a multiphase microstructure consisting of austenite, bainitic ferrite, and tempered martensite. The quench temperature was found to have a significant effect on the phase volume fractions. The lowest austenite volume fraction, approximately 26%, was observed in the sample quenched at 110°C, which also displayed the highest martensite content, as predicted by Koistinen-Marburger (K-M) equation. As the quenching temperature increased, the martensite volume fraction decreased, while the austenite fraction increased. All Q&P-treated samples demonstrated enhanced wear resistance compared to the as-cast condition. Notably, the sample quenched at 110°C exhibited the lowest weight loss, the lowest average coefficient of friction value of 0.64, and the highest hardness value of 458 HBW, along with the lowest wear rate of 21(m3(N.m)−1×10−15) and wear loss of 60 × 10−4 g.