EFFICIENT DETERMINATION AND PESTICIDE CONTROL BY MEANS OF IMMOBILIZATION OF ACETYLCHOLINESTERASE


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Ozkan E. H. , Yetim N. K. , Gumus M., SARI N. , DİŞLİ A.

MACEDONIAN JOURNAL OF CHEMISTRY AND CHEMICAL ENGINEERING, cilt.36, ss.119-128, 2017 (SCI İndekslerine Giren Dergi) identifier

  • Cilt numarası: 36 Konu: 1
  • Basım Tarihi: 2017
  • Doi Numarası: 10.20450/mjcce.2017.1178
  • Dergi Adı: MACEDONIAN JOURNAL OF CHEMISTRY AND CHEMICAL ENGINEERING
  • Sayfa Sayıları: ss.119-128

Özet

Supports involving tetrazole (o/m/p-F-Tet-1H) were prepared to detect pesticides. This novel tetrazole including fluorine in different positions was attached to nanoparticles (2AEPS-(o/m/p-F-Tet-1H)) by a condensation method. Primarily, the tetrazole derivatives were characterized by H-1-NMR, C-13-NMR and LC-MS. Then, nanoparticles were prepared by a condensation method in non-aqueous medium and characterized by Fourier transform infrared spectroscopy, scanning electron microscopy, gel permeation chromatography. The enzymatic properties of immobilized acetylcholinesterase (AChE) were investigated for the determination of phosmet. This research is the first example.