EFFICIENT DETERMINATION AND PESTICIDE CONTROL BY MEANS OF IMMOBILIZATION OF ACETYLCHOLINESTERASE


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Hasanoğlu Özkan E. , Kurnaz Yetim N., Gümüş M., Sarı N. , Dişli A.

MACEDONIAN JOURNAL OF CHEMISTRY AND CHEMICAL ENGINEERING, vol.36, pp.119-128, 2017 (Journal Indexed in SCI) identifier

  • Publication Type: Article / Article
  • Volume: 36
  • Publication Date: 2017
  • Doi Number: 10.20450/mjcce.2017.1178
  • Title of Journal : MACEDONIAN JOURNAL OF CHEMISTRY AND CHEMICAL ENGINEERING
  • Page Numbers: pp.119-128

Abstract

Supports involving tetrazole (o/m/p-F-Tet-1H) were prepared to detect pesticides. This novel tetrazole including fluorine in different positions was attached to nanoparticles (2AEPS-(o/m/p-F-Tet-1H)) by a condensation method. Primarily, the tetrazole derivatives were characterized by H-1-NMR, C-13-NMR and LC-MS. Then, nanoparticles were prepared by a condensation method in non-aqueous medium and characterized by Fourier transform infrared spectroscopy, scanning electron microscopy, gel permeation chromatography. The enzymatic properties of immobilized acetylcholinesterase (AChE) were investigated for the determination of phosmet. This research is the first example.