Copy For Citation
YAVUZ S., ÖZKAN H., ÇOLAK N., YILDIRIR Y.
MOLECULES, vol.16, no.8, pp.6677-6683, 2011 (SCI-Expanded)
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Publication Type:
Article / Article
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Volume:
16
Issue:
8
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Publication Date:
2011
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Doi Number:
10.3390/molecules16086677
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Journal Name:
MOLECULES
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Journal Indexes:
Science Citation Index Expanded (SCI-EXPANDED), Scopus
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Page Numbers:
pp.6677-6683
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Keywords:
nitrone, grinding, solid-phase synthesis, solventless, SOLVENT-FREE SYNTHESIS, CYCLOADDITION REACTIONS, EFFICIENT, OXIDATION, MICROWAVE
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Gazi University Affiliated:
Yes
Abstract
A simple, fast, efficient and eco-friendly procedure was developed for the synthesis of alkyl and aryl-N-methylnitrones. The corresponding nitrones of aromatic aldehydes, aliphatic aldehydes and alicyclic carbonyl compounds were prepared from N-methylhydroxylamine hydrochloride and Na2CO3-Na2SO4 by simply grinding at room temperature without using solvent.