Fast Method for Synthesis of Alkyl and Aryl-N-Methylnitrones


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YAVUZ S. , ÖZKAN H., ÇOLAK N., YILDIRIR Y.

MOLECULES, cilt.16, ss.6677-6683, 2011 (SCI İndekslerine Giren Dergi) identifier identifier identifier

  • Cilt numarası: 16 Konu: 8
  • Basım Tarihi: 2011
  • Doi Numarası: 10.3390/molecules16086677
  • Dergi Adı: MOLECULES
  • Sayfa Sayıları: ss.6677-6683

Özet

A simple, fast, efficient and eco-friendly procedure was developed for the synthesis of alkyl and aryl-N-methylnitrones. The corresponding nitrones of aromatic aldehydes, aliphatic aldehydes and alicyclic carbonyl compounds were prepared from N-methylhydroxylamine hydrochloride and Na2CO3-Na2SO4 by simply grinding at room temperature without using solvent.