You can see your results from this link
ilk beş deneyin video linki: https://drive.google.com/drive/folders/1At1DFzjvAtuIRITIqNZuFl06dFVTMxSo?usp=sharing
2024-2025 GÜZ DÖNEMİ KİMYA MÜH.
KİM 213 ANALİTİK KİMYA LAB. PROGRAMI
HAFTA | TARİH | DENEYİN ADI |
|
1 | 23-24 Eylül | Laboratuvar dersi ile ilgili genel kurallar ve uygulamalar hakkında bilgilendirme |
|
2 | 30 Eylül-1 Ekim | 1. Grup Katyonların Analizi | NİTEL (KALİTATİF) ANALİZ |
3 | 7-8 Ekim | 2. Grup Katyonların Analizi | |
4 | 14-15 Ekim | 3. Grup Katyonların Analizi | |
5 | 21-22 Ekim | 4. ve 5. Grup Katyonların Analizi | |
6 | 28-29 Ekim | Cumhuriyet Bayramı | |
7 | 4-5 Kasım | Genel Katyon Analizi | |
8 | 11-12 Kasım | Telafi Haftası | |
9 | 18-19 Kasım | Asit Baz Titrasyonu (Sirkede Asetik Asit Tayini) | NİCEL (KANTİTATİF) ANALİZ |
10 | 25-26 Kasım | Volhard Metoduyla Klorür Tayini | |
11 | 2-3 Aralık | EDTA ile Suda Sertlik Tayini-Potasyum Permanganat Çözeltisinin Hazırlanması | |
12 | 9-10 Aralık | Redoks Tepkimesiyle Kalsiyum Tayini | |
13 | 16-17 Aralık | İyodometrik Yöntemle Bakır Tayini | |
14 | 23-24 Aralık | Telafi Haftası | |
15 | 30-31 Aralık | Telafi Haftası |
LABORATUVARDA UYGULANACAK KURALLAR
1- Önlüğü, koruyucu laboratuvar gözlüğü, ve eldiveni olmayan öğrenci laboratuvara alınmayacaktır.
2- Her hafta deneyle ilgili deneyden önce küçük sınav yapılır.
3- Deneyden geçme notu 40’dır, 40’ın altında not alanlar o deneyden telafiye kalır. En fazla 3 deneyden telafiye kalınabilir. Daha fazla sayıda deneyden telafiye kalan öğrenci başarısız sayılır. Telafiye kalınan deneyler telafi haftasında tekrarlanır.
4- Laboratuvar ara sınav notu deney notu ortalamasının % 60’ı ile küçük sınav notu ortalamasının % 40’ı toplanarak bulunur.
5- Geçme notu Laboratuvar ara sınav notunun % 60 ve Final notunun % 40’ı toplanarak hesaplanır.
6- Nitel Analizde Deney notu: [(Doğru bulunan Katyon Sayısı) /(Verilen Katyon Sayısı +Yanlış Bulunan Katyon Sayısı)] x 100
formülüyle hesaplanır.
Nicel Analizde Deney notu: Öğrencinin yaptığı % Hataya göre değerlendirilir.
Doç. Dr. Demet UZUN
MATERIALS TO BE SUPPLIED BY STUDENTS (ÖĞRENCİLER TARAFINDAN ALINACAK MALZEMELER)
· Laboratory coat, goggles, nitrile gloves, scientific calculator, labels, acetate markers (Laboratuvar önlüğü, gözlük, nitril eldiven, bilimsel hesap makinası, etiket, asetat kalemi)
· Cleaning cloth, detergent etc., as a group (Temizlik bezi, deterjan vb., grup halinde)
· 10 pieces of centrifuge tubes (10 adet santrifüj tüpü)
· 10 pieces of 15 cm test tubes (10 adet 15 cm deney tüpü)
· Tube brush (Tüp fırçası)
· 3 pieces of 100 mL glass bottles with dropper (3 adet 100 mL’lik damlalıklı cam şişe)
· 15 pieces of plastic Pasteur pipettes (15 adet plastik Pastör pipeti)
· Puar, as a group (Puar, grup halinde)
· Evaporating dish (Porselen kapsül)
· 3 cm long platinum wire with an additional glass baguette, for the whole section (tüm şube için 1 adet 3 cm uzunluğunda platin tel, ayrıca bir adet cam baget ile birlikte)
First 5 experiments videos link: https://drive.google.com/drive/folders/1At1DFzjvAtuIRITIqNZuFl06dFVTMxSo?usp=sharing
2024-2025 FALL
SEMESTER CHEMICAL ENGINEERING. Sectıon 1 (Monday)
CHEM 213 ANALYTICAL
CHEMISTRY LAB. PROGRAM
|
Week |
|
EXPERIMENTS |
|
|
1 |
23rd SEPT |
General
Information and Informing the Student |
|
|
2 |
30th SEPT |
Analysis
of Group I Cations |
QUALITATIVE ANALYSIS |
|
3 |
7th OCT |
Analysis
of Group II Cations |
|
|
4 |
14th OCT |
Analysis
of Group III Cations |
|
|
5 |
21th OCT |
Analysis
of Group IV-V Cations |
|
|
6 |
28th OCTOBER |
|
|
|
7 |
4th NOV |
General
Cation Analysis |
|
|
8 |
11th NOV |
MAKE
UP |
QUANTITATIVE
ANALYSIS |
|
9 |
18th NOV |
Acid
Base Titrations-Determination of Acetic acid in Vinegar. |
|
|
10 |
25st NOV |
Precipitation
Titrations-Chloride Determination by Volhard Method |
|
|
11 |
2nd DEC |
Complexometric
Titrations-Determination of Hardness of
Water with EDTA |
|
|
12 |
9th DEC |
Redox
titrations-Ca(II) Determination by Redox Titration with KMnO4 |
|
|
13 |
16th DEC |
Iodometric
Titration-Copper (II) Determination |
|
|
14 |
23th DEC |
MAKE-UP |
|
|
15 |
30th JAN |
MAKE
UP |
|
2024-2025 FALL SEMESTER CHEMICAL ENGINEERING. SECTION 2 (WEDNESDAY)
CHEM 213 ANALYTICAL CHEMISTRY LAB. PROGRAM
|
Week |
|
EXPERIMENTS |
|
|
1 |
25rd
SEPT |
General Information and Informing the Student |
|
|
2 |
2nd
OCT |
Analysis of Group I Cations |
QUALITATIVE
ANALYSIS |
|
3 |
9th
OCT |
Analysis of Group II Cations |
|
|
4 |
16th
OCT |
Analysis of Group III Cations |
|
|
5 |
23th
OCT |
Analysis of Group IV-V Cations |
|
|
6 |
28th OCTOBER |
|
|
|
7 |
6th
NOV |
General Cation Analysis |
|
|
8 |
13th
NOV |
MAKE UP |
QUANTITATIVE ANALYSIS |
|
9 |
20th
NOV |
Acid Base Titrations-Determination of Acetic
acid in Vinegar. |
|
|
10 |
27st
NOV |
Precipitation Titrations-Chloride
Determination by Volhard Method |
|
|
11 |
4nd
DEC |
Complexometric Titrations-Determination of
Hardness of Water with EDTA |
|
|
12 |
11h
DEC |
Redox titrations-Ca(II) Determination by Redox
Titration with KMnO4 |
|
|
13 |
18th
DEC |
Iodometric Titration-Copper (II) Determination |
|
|
14 |
25th
DEC |
MAKE-UP |
|
|
15 |
30th
DEC |
MAKE-UP(with section 1) |
|
RULES TO BE APPLIED IN THE LABORATORY
1- It is imperative to wear a
lab coat. A student without a lab coat will not be allowed to enter the
laboratory.
2- Before starting the
experiment every week, a quiz will be taken from the relevant experiment.
3- You need to get at least 40
points from the experiment. Those who take notes below 40 points are considered
unsuccessful in that experiment. Up to 3 experiments can be compensated.
The student who fails to compensate for the larger number of attempts is deemed
unsuccessful. Failed experiments are repeated in the make-up week.
4- Laboratory grade is calculated
by adding 30% of the average of the experimental study grade and 30% of the
average grade of the quiz-examination and 40% of the final exam grade.
5- In Qualitative Analysis-section,
the experimental grade is calculated as follows:
[(Number of Cations Found Correctly) / (Number of Cations Given + Number
of Cations Incorrect)] x 100
In Quantitative Analysis-section,
the experimental grade is calculated as follows:
{ 100 - [% Error x (100 - 40)] / Compensation Limit}.
(Compensation limit is
determined separately for each experiment)
Prof. Dr. Recai İNAM
MATERIALS TO BE SUPPLIED BY STUDENTS (ÖĞRENCİLER TARAFINDAN ALINACAK MALZEMELER)
· Laboratory coat, goggles, nitrile gloves, scientific calculator, labels, acetate markers (Laboratuvar önlüğü, gözlük, nitril eldiven, bilimsel hesap makinası, etiket, asetat kalemi)
· Cleaning cloth, detergent etc., as a group (Temizlik bezi, deterjan vb., grup halinde)
· 10 pieces of centrifuge tubes (10 adet santrifüj tüpü)
· 10 pieces of 15 cm test tubes (10 adet 15 cm deney tüpü)
· Tube brush (Tüp fırçası)
· 3 pieces of 100 mL glass bottles with dropper (3 adet 100 mL’lik damlalıklı cam şişe)
· 15 pieces of plastic Pasteur pipettes (15 adet plastik Pastör pipeti)
· Puar, as a group (Puar, grup halinde)
· Evaporating dish (Porselen kapsül)
· 3 cm long platinum wire with an additional glass baguette, for the whole section (tüm şube için 1 adet 3 cm uzunluğunda platin tel, ayrıca bir adet cam baget ile birlikte)
NOTE
• For
calculations in the experiment, all students must bring calculators.
•
Always keep the laboratory sheets with you.
https://drive.google.com/drive/folders/1zrQ2Go4tqetPWRIS_hIyxqTCBbD1N1lz?usp=sharing
HyberChem Program linki yukarıda yazılmıştır.
Laboratuvar kuralları aşağıdaki dosyada bulunmaktadır.
Rapor formları ilgili deneyin asistan hocası tarafından verilecektir. https://drive.google.com/drive/folders/1UssK7DzIRZYsf-mSur6tkOcHA8yWW42r?usp=sharing
Deney föyleri https://drive.google.com/drive/folders/167wo9XV74R7yGQggKvLVwG-2bMyTz_l4?usp=sharing linkinde bulunmaktadır.
Deney linkleri sırasıyla;
Moleküler Modelleme I
https://drive.google.com/file/d/1yaUz2CgqkVGJDmFAmVB3WxybT3ungbIs/view?usp=sharing
Bağlanma İzomerliği
https://drive.google.com/file/d/16YyIikMHt6z93fUXsq_DSCfsGjygITqL/view?usp=sharing
Kalay İyodürler
https://drive.google.com/file/d/1KOjJUevhGQjthp7qabnxCeeiUfDdDb4y/view?usp=sharing
Manyetizma
https://drive.google.com/file/d/1EeNHF4clizjfiTTxllkA3LTP1Q22CIY4/view?usp=sharing
Metal Okzalatlar
https://drive.google.com/file/d/185cw9nWP29siLVyMliGv8UKnq1IdFRad/view?usp=sharing
İnert Çift Etkisi
https://drive.google.com/file/d/1xju2QL8q7vWOPGlWxOo_V_VoAYmBl69T/view?usp=sharing
Moleküler Modelleme II
https://drive.google.com/file/d/1iYv85rHN7bEjKghvZWOBcxEvGG9u-_nF/view?usp=sharing
Geometrik İzomerlik
https://drive.google.com/file/d/1rySEqiF7hPSVxHVtWrEL80LX-y5XWdus/view?usp=sharing
Kinetik
https://drive.google.com/file/d/1-xO6BoJkNx_rdvT0PrrRvD_teeKKIyUS/view?usp=sharing
KAYE
https://drive.google.com/drive/folders/1qYYXge5zQ0r2we0vqvBMpBm-PwtcprTs?usp=sharing